WitrynaThe flask is charged with 100 mL of tetrahydrofuran and 2.16 g (57.0 mmol) of lithium aluminum hydride (Note 6) and (Note 13). While the suspension in the flask is … WitrynaThe product is dried to constant weight over Drierite in a vacuum desiccator to yield 27-28 g of a white solid. This material is recrystallized (three times) by dissolving it in 175 …

Hypervalent Iodine Compounds SpringerLink

http://orgsyn.org/demo.aspx?prep=v97p0157 http://www.orgsyn.org/demo.aspx?prep=V77P0001 meatball mr

Organic Syntheses Procedure

WitrynaThe flask is charged with indole (3.51 g, 30.0 mmol) (Note 11), and then the resulting dark red suspension is stirred at 25 °C for 4 hr. The mixture is removed from the oil … WitrynaThe wet cake (Note 10) is transferred to a mixture of 100 mL of heptane and 138 mL of 2 M sodium hydroxide (NaOH) with stirring (Note 11).The two layers are separated. The aqueous layer (pH > 12) is extracted with heptane (75 mL).The combined organic layers are washed with water (50 mL), filtered through a cotton wool plug and concentrated … Witryna'Hypervalent Iodine Compounds' published in 'Oxidation of Alcohols to Aldehydes and Ketones' meatball mummies